GCMS Analysis Report for Sample AD26386, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26386.D Vial: 12 Acq On : 30 Nov 2001 10:13 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise 2 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Hydrogen azide Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T. 5.01 1.30 ng/uL 580103 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 entative ID MW MolForm CAS# Qual

1 Hydrogen azide 43 HN3 007782-79-8 4 2 Acetic acid, anhydride 102 C4H603 000108-24-7 2 3 Acetic acid, anhydride 102 C4H603 000108-24-7 2 4 Acetic acid, 2-methylpropyl ester 116 C6H12O2 000110-19-0 2 Abundance Scan 19 (5.013 min): 26386.D (-) m/z 43.00 100.00% 43

5000 -= m

4.90 5.00 5.10 5.20 5.30 5.40 ------ 11 >! <. TIITTITT 55 83 87 m/z42.00 6.53% ‘I ।।। TTHI] 11 mz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #33: Hydrogen azide 43

5000 15 4.90 5.00 5.1 5.20 6.30 5.40

29 m/z . 44.00 2.92% 111" — mm —।।. Hmmmmmmmm — wpmmp m miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63470: Acetic acid, anhydride 43 I 114)—t**]t***otsitrt1119931r 4.90 5.00 5.1 5.20 5.30 5.40 5000 m/z 41. 0 1.36%

15 _______ ,_______ 29_______ , ,_________ 60 ............................ 87 I ] I I 1 . | H I I | I I I I | IT-H | U I fj . . . . | . TTI 1117 TIIUT TIT | | | |. miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #1680: Acetic acid, anhydride 48 4.90 5.00 5.10 5.20 5.30 5.40 m/z 45.00 0.91% 5000

_____________ 29______ . ,________ 60 87 ‘I1 T1-mm02n]—n-—mmmp11111_uD1111111711111E10T1141 —TIMIPTTTf miz—> 5 10 15 202530 35 404550556065 70 75 80859095 4.90 5.00 5.10 5.20 5.30 5.40

26386.D NP112701.M Tue Dec 04 10:38:32 2001 Page 1

NYC-WTC_000031423