GCMS Analysis Report for Sample AD26386, Dec 2001

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26386.D vial: 12 Acq On : 30 Nov 2001 10:13 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise 2 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopropane, (1-methylethyl)- Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 5.10 0.82 ng/uL 365882 1,4-Dichlorobenzene-d4 11.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopropane, (1-methylethyl)- 84 C6H12 003638-35-5 10 2 Ethane, diazo- 56 C2H4N2 001117-96-0 9 3 2-Butene, (E) - 56 C4H8 000624-64-6 9 4 2-Butene 56 C4H8 000107-01-7 9 Abundance C Scan 28 (5.095 min): 26386.D (-) m/z 41.05 100.00% 41 5659

5000

38 ■ ■ । • ■ ‘ ■ i ■1 ■ ■ i ■ ■ ■ • i • ■ ■ ■ i ■ ■ ■ ■ i ■ ■ > ■ ।111 45

m 51 1 , 67 71

Tp TIU_TDI . N.... 4.90 5.00 5.10 5.20 5.30 5.40 5.50 m/z 56.10 79.07% m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #592: Cyclopropane, (1-methylethyl)- 56 41

5000 Tmmgm 4.90 5.00 5.10 5.20 5.30 5.40 5.50 27 m/z 59.10 76.29% 15 69 TmDT 111 ■ ■11137 50 53 ,I.. (. i. ।. 1111|.................. TTTeptuHr 84 n 11111! 11 ■ 11111111111, 1' ■' I miz-> 5 10 15 20 25 3035404550556065 70 75808590 Abundance #71: Ethane, diazo- 27

D .. 1111111111।: 111111111:111 ((1111 ri 56 4.90 5.00 5.10 5.20 5.30 5.40 5.50 5000 m/z 42.00 64.89%

5053, ।।।i > 11. i < | l ।....।.1111ri11111111111 miz-> 5 10 15 20253035404550556065 70 75 808590 Abundance #62302 2-Butene, (E)- 41 4.90 5.00 5.10 5.20 5.30 5.40 5.50 m/z 43.05 59.30% 56 5000 27

1 30 TITH 38 । , 4952, uummmunPpTr Inpm p m/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 4.90 5.00 5.10 5.20 5.30 5.40 5.50

26386.D NP112701.M Tue Dec 04 10:38:33 2001 Page 2

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