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GCMS non-target scan comment, Dec 2001

Machine-extracted title · confidence 90%

Laboratory comment confirming no non-target compounds were detected in sample AD26203 on December 10, 2001.

NYC-WTC_000031359–000031371

Folder label: “GCMS X 11/5/01 A 12/1/01

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NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\NOV3001\26203.D Vial: 26 Acq On 1 Dec 2001 10:56 am Operator: GALOS Sample : gc/ms unknown 11/3 reext Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 4.937 5 10 15 rBV 58409 106972 1.45% 0.295% 2 5.010 15 18 23 rBV 68334 121906 1.65% 0.337% 3 5.166 32 35 49 rVB3 31187 123186 1.67% 0.340% 4 6.560 184 187 198 rW 37004 88572 1.20% 0.245% 5 7.165 249 253 266 rBV 172656 340726 4.61% 0.941%

6 7.844 323 327 336 rBV 560528 1177510 15.92% 3.251% 7 7.935 336 337 346 rVB 88933 76484 1.03% 0.211% 8 10.320 593 597 604 rBV 66416 129940 1.76% 0.359% 9 10.531 616 620 629 rBV 51959 107263 1.45% 0.296% 10 11.888 762 768 786 rBV 2870485 6030221 81.51% 16.651% .

11 15.5011 1156 1162 1180 rBV 3603659 7398350 100.00% 20.429% 12 20.774 1731 1737 1754 rBV 3540524 7202340 97.35% 19.888% 13 25.184 2211 2218 2229 rBV2 2867045 6241998 84.37% 17.236% 14 33.181 3084 3090 3106 rBV2 1753385 3990164 53.93% 11.018% 15 37.271 3529 3536 3550 rBV 1165031 3079180 41.62% 8.503%

Sum of corrected areas: 36214812 26203.D 112701.M Tue Dec 04 15:05:55 2001

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NYC-WTC_000031365Source: NYC Law Department, mirrored locally

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