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GCMS results log, sample AD26983, Dec 11 2001

Machine-extracted title · confidence 100%

Laboratory report for GCMS analysis of sample AD26983 completed on December 11, 2001, with surrogate recovery data.

NYC-WTC_000032362–000032377

Folder label: “GCMS X 11/8/01 A 12/7/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\DEC0 601\26983.D Vial: 25 Acq On 7 Dec 2001 7:59 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 5.037 13 21 26 rBV 105659 195594 2.17% 0.429% 2 5.147 30 33 37 rBV 85638 146795 1.63% 0.322% 3 5.211 37 40 46 rVB 120422 204022 2.27% 0.447% 4 6.138 137 141 154 rBV 84329 191338 2.13% 0.419% 5 6.477 173 173 187 rBV 56186 121759 1.35% 0.267%

6 6.587 187 190 2 00 rW 7 0 942 160160 1.78% 0.351% 7 6.825 213 216 226 rW2 51872 111600 1.24% 0.245% 8 7.861 326 329 341 rBV 146355 321517 3.57% 0.704% 9 10.319 590 597 605 rBV 105021 194599 2.16% 0.426% 10 10.530 614 620 629 rBV 62306 122871 1.36% 0.269%

11 11.887 763 768 782 rBV 3548983 7201248 79.98% 15.777% 12 15.500 1155 1162 1181 rBV 4306152 9003284 100.00% 19.725% 13 20.773 1731 1737 1753 rBV 4336341 8747665 97.16% 19.165% 14 25.184 2211 2218 2229 rBV2 3780874 8101008 89.98% 17.748% 15 25.321 2229 2233 2244 rVB3 31631 103148 1.15% 0.226%

16 33.189 3084 3091 3115 rBV2 2610218 5914189 65.69% 12.957% 17 37.270 3527 3536 3556 rBV2 1731645 4803063 53.35% 10.523%

Sum of corrected areas: 45643860

26983 .D NP112701 .M Tue Dec 11 14:49:27 2001

NYC-WTC_000032368

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NYC-WTC_000032368Source: NYC Law Department, mirrored locally

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