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GCMS results log, sample AD27007, Dec 11 2001

Machine-extracted title · confidence 100%

Laboratory report for GCMS analysis of sample AD27007 completed on December 11, 2001.

NYC-WTC_000032503–000032519

Folder label: “GCMS X 11/8/01 A 12/7/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

' Data File C:\HPCHEM\1\DATA\DEC0601\27007.D Vial: 22 Acq On 7 Dec 2001 5:16 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 5.025 13 20 30 rVB 96825 200657 2.43% 0.451% 2 6.584 186 190 201 rVB 55180 125388 1.52% 0.282% 3 7.850 324 328 346 rVB 562632 1195317 14.48% 2.686% 4 10.683 636 637 639 rBV 163272 95965 1.16% 0.216% 5 11.894 763 769 787 rBV 3106696 6681028 80.91% 15.014%

6 15.497 1156 1162 1180 rBV 3833431 8257332 100.00% 18.556% 7 20.779 1731 1738 1752 rBV 3731781 8119855 98.34% 18.247% 8 25.181 2212 2218 2230 rBV2 3462486 7647014 92.61% 17.184% 9 29.592 2693 2699 2706 rBV 99296 211059 2.56% 0.474% 10 29.702 2706 2711 2721 rVB2 40483 89126 1.08% 0.200%

11 30.775 2824 2828 2836 rVB 45917 102778 1.24% 0.231% 12 31.719 2925 2931 2936 rBV 55028 135527 1.64% 0.305% 13 31.802 2936 2940 2952 rVB 102753 267119 3.23% 0.600% 14 32.801 3042 3049 3062 rBV 73320 217517 2.63% 0.489% 15 33.187 3085 3091 3109 rBV2 2621000 5846198 70.80% 13.138%

16 33.746 3147 3152 3162 rBV 71559 225165 2.73% 0.506% 17 34.663 3247 3252 3261 rBV2 35010 118769 ' 1.44% 0.267% 18 35.552 3343 3349 3360 rBV2 24676 90181 1.09% 0.203% 19 37.276 3529 3537 3558 rBV2 1752676 4874029 59.03% 10.953%

Sum of corrected areas: 44500024

27007.D NP112701.M Tue Dec 11 14:56:31 2001

NYC-WTC_000032509

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NYC-WTC_000032509Source: NYC Law Department, mirrored locally

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