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GCMS results log, sample AD26982, Dec 11 2001

Machine-extracted title · confidence 100%

Laboratory report for GCMS analysis of sample AD26982 completed on December 11, 2001, noting unknown compounds.

NYC-WTC_000032343–000032361

Folder label: “GCMS X 11/8/01 A 12/7/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\DEC0601\26982.D Vial: 24 Acq On 7 Dec 2001 7:05 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 5.046 15 22 31 rVB 117155 220909 2.11% 0.378% 2 5.156 31 34 38 rBV 204743 344128 3.29% 0.588% 3 5.220 38 41 47 rVB 260280 450827 4.31% 0.771% 4 6.137 138 141 154 rVB 167009 368145 3.52% 0.629% 5 6.486 175 179 187 rBV 72300 146172 1.40% 0.250%

6 6.596 187 191 201 rVB 78112 162912 1.56% 0.278% 7 6.724 201 205 213 rBV 52298 107162 1.02% 0.183% 8 6.834 213 217 223 rBV2 45661 108042 1.03% 0.185% 9 7.183 247 255 263 rBV 410038 932184 8.91% 1.593% 10 7.852 324 32 8 346 rVB 578623 1244482 11.90% 2.127%

11 10.319 592 597 604 rBV 233098 449783 4.30% 0.769% 12 10.530 613 620 629 rBV 127814 248918 2.38% 0.425% 13 11.887 762 768 781 rBV 4145098 8300527 79.35% 14.188% 14 15.500 1155 1162 1179 rBV 4874156 10460441 100.00% 17.879% 15 20.773 1730 1737 1756 rBV 4976717 10412500 99.54% 17.797%

16 25.184 2211 2218 2230 rBV2 4526263 9757888 93.28% 16.679% 17 31.805 2934 2940 2950 rVB 69216 171797 1.64% 0.294% 18 32.795 3043 3048 3056 rBV2 50939 145703 1.39% 0.249% 19 33.189 3084 3091 3114 rBV2 3482387 7788973 74.46% 13.313% 20 33.749 3146 3152 3162 rBV3 51699 162627 1.55% 0.278%

21 37.279 3529 3537 3556 rBV2 2340530 6521345 62.34% 11.147%

Sum of corrected areas: 58505465

26982.D NP112701.M Tue Dec 11 14:48:37 2001

NYC-WTC_000032349

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NYC-WTC_000032349Source: NYC Law Department, mirrored locally

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