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GCMS analysis results for sample AD26625, Dec 10 2001

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Laboratory report documenting GCMS analysis of sample AD26625 identifying unknown compounds on December 10, 2001.

NYC-WTC_000031920–000031939

Folder label: “GCMS X 11/7/01 A 12/6/01

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Scanned page image, NYC-WTC_000031925
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\DEC0601\26625.D Vial: 8 Acq On 6 Dec 2001 4:34 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 5.014 12 19 28 rBV 130861 515744 6.42% 1.069% 2 5.124 28 31 35 rW 258408 471635 5.87% 0.978% 3 5.188 35 38 56 rVB 373996 907764 11.31% 1.882% 4 5.665 87 90 98 rVB 52391 110041 1.37% 0.228% 5 6.123 136 140 153 rVB 209157 534735 6.66% 1.109%

6 6.472 174 178 186 rBV 83912 188108 2.34% 0.390% 7 6.573 186 189 200 rVB 84880 208816 2.60% 0.433% 8 6.701 200 203 212 rBV2 81173 232354 2.89% 0.482% 9 6.820 212 216 220 rBV2 56833 109414 1.36% 0.227% 10 7.178 246 255 274 rVB 995399 2096232 26.11% 4.346%

11 7.847 324 328 343 rBV 1303136 2772176 34.53% 5.747% 12 10.314 593 597 605 rBV 355894 724345 9.02% 1.502% ' 13 10.525 615 620 631 rBV 191287 383907 4.78% 0.796% 14 11.882 763 768 782 rBV 3118260 6462817 80.49% 13.398% 15 15.495 1156 1162 1181 rBV 3865515 8029244 100.00% 16.645%

16 20.768 1731 1737 1757 rBV 3821247 8018774 99.87% 16.624% 17 25.179 2212 2218 2230 rBV2 3341158 7238355 90.15% 15.006% 18 25.316 2230 2233 2246 rVB2 28360 89483 1.11% 0.186% 19 33.184 3084 3091 3109 rBV2 2289624 5054174 62.95% 10.478% 20 33.450 3114 3120 3133 rVB2 52653 141240 1.76% 0.293%

21 37.274 3529 3537 3552 rBV2 1467655 3947945 49.17% 8.184%

Sum of corrected areas: 48237303

26625.D NP112701.M Fri Dec 07 14:48:25 2001

NYC-WTC_000031925

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NYC-WTC_000031925Source: NYC Law Department, mirrored locally

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