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GCMS analysis sample AD26538, unknown compounds, Dec 2001

Machine-extracted title · confidence 80%

GC/MS analysis of sample AD26538 identified other unknown compounds noted in comments section, December 10, 2001.

NYC-WTC_000031889–000031904

Folder label: “GCMS X 11/7/01 A 12/6/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\DEC0601\26538 . D Vial: 13 Acq On 6 Dec 2001 9:06 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 5.069 21 25 35 rBV 628009 1470278 21.47% 3.440% 2 6.132 137 141 148 rBV 22059 74391 1.09% 0.174% 3 6.490 175 180 188 rBV 31525 99390 1.45% 0.233% 4 6.600 188 192 201 rVB 30191 73174 1.07% 0.171% 5 6.719 201 205 208 rBV 45112 103771 1.52% 0.243%

6 6.839 214 218 225 rVB 33191 81449 1.19% 0.191% 7 7.215 253 259 276 rVB 2031629 3997927 58.37% 9.354% 8 7.866 326 330 347 rBV 1130085 2462588 35.95% 5.762% 9 9.379 490 495 503 rBV 110171 234532 3.42% 0.549% 10 9.626 517 522 536 rVB2 206612 748252 10.92% 1.751% 11 10.332 595 599 608 rBV 61478 128602 1.88% 0.301% 12 10.543 618 622 630 rBV 56397 119273 1.74% 0.279% 13 11.891 763 769 788 rBV 2690272 5575415 81.40% 13.045% 14 15.504 1157 1163 1181 rBV 3289334 6849139 100.00% 16.025% 15 20.768 1731 1737 1762 rBV 3227320 6737964 98.38% 15.764%

16 25.179 2212 2218 2230 rBV2 2698862 6058770 88.46% 14.175% 17 33.184 3085 3091 3105 rBV2 1968566 4486513 65.50% 10.497% 18 33.450 3116 3120 3131 rVB 48268 127435 1.86% 0.298% 19 37.274 3529 3537 3561 rBV2 1205468 3312600 48.37% 7.750%

Sum of corrected areas: 42741463

26538.D NP112701.M Fri Dec 07 14:46:59 2001

NYC-WTC_000031893

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NYC-WTC_000031893Source: NYC Law Department, mirrored locally

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