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GCMS analysis results for sample AD26828, Dec 10 2001

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Laboratory report documenting GCMS analysis of sample AD26828 identifying unknown compounds on December 10, 2001.

NYC-WTC_000032182–000032201

Folder label: “GCMS X 11/7/01 A 12/6/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report •

Data File C:\HPCHEM\l\DATA\DEC0601\26828.D Vial: 12 Acq On 6 Dec 2001 8:12 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 5.004 11 18 27 rBV2 90113 322166 5.25% 0.900% 2 5.114 27 30 34 rW 179039 334885 5.46% 0.936% 3 5.178 34 37 56 rVB 273961 748070 12.19% 2.090% 4 5.664 86 90 96 rVB 34961 82783 1.35% 0.231% 5 6.113 135 139 155 rBV 153609 412454 6.72% 1.152%

6 6.462 174 177 184 rBV 55025 124390 2.03% 0.348% 7 6.572 186 189 199 rVB 56562 127467 2.08% 0.356% 8 6.700 199 203 212 rBV 49722 107084 1.74% 0.299% 9 6.819 212 216 222 rBV2 32473 72257 1.18% 0.202% 10 7.168 248 254 267 rBV 522876 1102370 17.96% 3.080%

11 7.837 324 327 344 rBV 711084 1616907 26.34% 4.518% 12 10.322 591 598 608 rBV 193267 437670 7.13% 1.223% 13 10.524 616 620 628 rBV 92243 196694 3.20% 0.550% 14 11.890 763 769 781 rBV 2335032 4993619 81.35% 13.952% 15 15.494 1157 1162 1181 rBV 2832649 6138659 100.00% 17.151%

16 20.767 1731 1737 1759 rBV 2865698 6105320 99.46% 17.058% 17 25.178 2212 2218 2230 rBV2 2513640 5517073 89.87% 15.415% 18 25.325 2230 2234 2242 rVB2 21712 64020 1.04% 0.179% 19 33.183 3085 3091 3106 rBV2 1779924 4032841 65.70% 11.268% 20 37.273 3530 3537 3552 rBV 1222802 3254240 53.01% 9.092%

Sum of corrected areas: 35790969

26828.D NP112701.M Fri Dec 07 14:53:10 2001

NYC-WTC_000032188

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NYC-WTC_000032188Source: NYC Law Department, mirrored locally

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