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GCMS analysis results for sample AD26680, Dec 10 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD26680 identifying unknown compounds on December 10, 2001.

NYC-WTC_000032058–000032078

Folder label: “GCMS X 11/7/01 A 12/6/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\DEC0401\26680.D Vial: 3 Acq On 4 Dec 2001 12:38 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 4.955 5 12 13 rBV 30661 77812 1.16% 0.198% 2 5.001 13 17 25 rW2 69856 226421 3.38% 0.576% 3 5.102 25 28 32 rW 226158 391502 5.84% 0.997% 4 5.166 32 35 55 rVB 331969 800198 11.94% 2.037% 5 5.652 85 88 100 rVB2 46296 123577 1.84% 0.315%

6 6.101 133 137 151 rBV 168379 425714 6.35% 1.084% 7 6.450 171 175 181 rBV 60714 121820 1.82% 0.310% 8 6.551 183 186 197 rVB 55879 136242 2.03% 0.347% 9 6.688 197 201 209 rBV 51263 126690 1.89% 0.323% 10 6.798 209 213 218 rBV2 38462 79995 1.19% 0.204%

11 7.147 245 251 265 rBV 623763 1382112 20.63% 3.519% 12 7.825 321 325 341 rBV 898727 1918294 28.63% 4.884% 13 10.301 590 595 604 rBV 209786 427498 6.38% 1.088% 14 10.512 612 618 626 rBV 82470 169676 2.53% 0.432% 15 11.869 760 766 779 rBV 2539420 5374756 80.23% 13.683%

16 15.482 1154 1160 1179 rBV 3123374 6699274 100.00% 17.055% 17 20.755 1729 1735 1749 rBV 3254216 6669609 99.56% 16.980% 18 25.166 2209 2216 2227 rBV2 2796923 6143482 91.70% 15.640% 19 33.162 3082 3088 3106 rBV2 2002992 4522301 67.50% 11.513% 20 33.428 3113 3117 3126 rVB 37139 86371 1.29% 0.220%

21 37.252 3525 3534 3551 rBV2 1276160 3376999 50.41% 8.597%

Sum of corrected areas: 39280343

26680.D NP112701.M Fri Dec 07 13:11:20 2001

NYC-WTC_000032063

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NYC-WTC_000032063Source: NYC Law Department, mirrored locally

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