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GCMS calibration table for TCLP analysis, Dec 5 2001

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Calibration data sheet listing standard compounds and response factors used for GCMS analysis on December 5, 2001.

NYC-WTC_000032142–000032159

Folder label: “GCMS X 11/7/01 A 12/6/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\DEC0501\26712.D Vial: 3 Acq On 5 Dec 2001 10:35 am Operator: GALOS Sample gc/ms unknown 11/7 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 5.010 7 18 26 rBV2 135619 552784 6.47% 1.170% 2 5 . ill 26 29 33 rW 203057 354684 4.15% 0.751% 3 5.175 33 36 53 rVB 300425 656290 7.68% 1.389% 4 6.110 134 138 150 rVB 153333 373184 4.37% 0.790% 5 6.450 171 175 184 rBV 60407 136893 1.60% 0.290%

6 6.560 184 187 191 rBV 71682 123644 1.45% 0.262% 7 6.688 197 201 203 rBV 58186 109413 1.28% 0.232% 8 6.807 210 214 219 rBV2 45450 96182 1.13% 0.204% 9 7.156 244 252 263 rBV 1072003 2288021 26.77% 4.842% 10 7.825 321 325 338 rBV 1511482 2861959 33.49% 6.057%

11 10.292 590 594 602 rBV 253543 513104 6.00% 1.086% 12 10.503 613 617 627 rBV2 136242 283922 3.32% 0.601% 13 11.860 759 765 782 rVB 3400770 6992465 81.81% 14.798% 14 15.473 1153 1159 1177 rBV 3900040 8546900 100.00% 18.088% 15 20.746 1728 1734 1752 rBV 3722602 8315576 97.29% 17.598%

16 25.166 2209 2216 2227 rBV2 3219215 7160404 83.78% 15.153% 17 33.162 3082 3088 3101 rBV2 2029317 4483585 52.46% 9.489% 18 33.428 3112 3117 3125 rVB 41403 95649 1.12% 0.202% 19 37.252 3526 3534 3547 rBV2 1222164 3308072 38.70% 7.001%

Sum of corrected areas: 47252731

26712.D NP112701.M Fri Dec 07 13:15:01 2001

NYC-WTC_000032146

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