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GCMS analysis results for sample AD26682, Dec 10 2001

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Laboratory report documenting GCMS analysis of sample AD26682 identifying unknown compounds on December 10, 2001.

NYC-WTC_000032093–000032113

Folder label: “GCMS X 11/7/01 A 12/6/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\DEC0501\26682.D Vial: 2 Acq On 5 Dec 2001 9:41 am Operator: GALOS Sample gc/ms unknown 11/7 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 4.991 13 16 22 rW 388140 720442 8.47% 1.559% 2 5.074 22 25 29 rW 145389 298217 3.51% 0.645% 3 5.138 29 32 55 rVB 226065 742323 8.73% 1.606% 4 6.082 131 135 139 rBV 117682 249468 2.93% 0.540% 5 6.431 169 173 181 rBV 84947 187117 2.20% 0.405%

6 6.541 181 185 195 rW 95065 204138 2.40% 0.442% 7 6.669 195 199 207 rW 76213 161913 1.90% 0.350% 8 6.789 208 212 217 rBV2 59960 123399 1.45% 0.267% 9 7.146 246 251 266 rVB 1202577 2130455 25.05% 4.609% 10 7.816 320 324 331 rBV 1364487 2647823 31.14% 5.728%

11 10.291 589 594 602 rBV 261828 536140 6.30% 1.160% 12 10.502 613 617 626 rBV 186083 366386 4.31% 0.793% 13 11.860 760 765 786 rBV 3320487 6892567 81.05% 14.912% 14 15.473 1153 1159 1177 rBV 4025570 8503769 100.00% 18.397% 15 20.745 1728 1734 1752 rBV 3726166 8129286 95.60% 17.587%

16 25.165 2209 2216 2227 rBV2 3119036 6979363 82.07% 15.099% 17 33.162 3082 3088 3104 rBV2 1975709 4312094 50.71% 9.329% 18 37.252 3526 3534 3549 rBV2 1109751 3037720 35.72% 6.572%

Sum of corrected areas: 46222620

26682.D NP112701.M Fri Dec 07 13:13:06 2001

NYC-WTC_000032099

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NYC-WTC_000032099Source: NYC Law Department, mirrored locally

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