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GCMS analysis results for sample AD26831, Dec 10 2001

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Laboratory report documenting GCMS analysis of sample AD26831 identifying unknown compounds on December 10, 2001.

NYC-WTC_000032232–000032244

Folder label: “GCMS X 11/7/01 A 12/6/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

• Data File C:\HPCHEM\1\DATA\DEC0501\26831.D Vial: 6 Acq On 5 Dec 2001 1:19 pm Operator: GALOS Sample gc/ms unknown 11/7 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 5.054 17 23 30 rVB 119485 223349 2.37% 0.500% 2 5.228 39 42 48 rW 70728 117374 1.24% 0.263% 3 6.145 138 142 150 rBV 50936 94649 1.00% 0.212% 4 6.484 171 179 185 rBV 55881 107788 1.14% 0.241% 5 6.585 186 190 199 rW 74786 153574 1.63% 0.344%

6 7.841 323 327 335 rBV 643427 1231478 13.04% 2.757% 7 10.299 590 595 604 rBV 79523 .143607 1.52% 0.321% 8 10.510 614 618 623 rBV 57093 107849 1.14% 0.241% 9 11.867 760 766 784 rVB 3570452 7456822 78.99% 16.691% 10 15.480 1152 1160 1177 rBV 3843132 9440301 100.00% 21.131%

11 20.753 1727 1735 1752 rBV 3996374 9244344 97.92% 20.692% 12 25.164 2208 2216 2228 rBV2 3613451 7932771 84.03% 17.757% 13 25.301 2228 2231 2245 rVB2 33019 97414 1.03% 0.218% 14 33.169 3082 3089 3107 rBV2 2168190 4731068 50.12% 10.590% 15 33.435 3113 3118 3128 rVB2 67009 153509 1.63% 0.344%

16 37.250 3527 3534 3550 rBV2 1261148 3439378 36.43% 7.699%

Sum of corrected areas: 44675275

26831.D NP112701.M Fri Dec 07 13:15:37 2001

NYC-WTC_000032238

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NYC-WTC_000032238Source: NYC Law Department, mirrored locally

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