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GCMS analysis results for sample AD26624, Dec 10 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD26624 identifying unknown compounds on December 10, 2001.

NYC-WTC_000031905–000031919

Folder label: “GCMS X 11/7/01 A 12/6/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

’ Data File C:\HPCHEM\1\DATA\DEC0601\26624.D Vial: 7 Acq On 6 Dec 2001 3:39 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % Of # min scan scan scan TY height area % max. total

1 5.064 20 24 33 rBV 262998 637773 11.26% 1.982% 2 7.201 252 257 271 rBV 918720 1729601 30.53% 5.376% 3 7.870 326 330 351 rBV 844086 1981853 34.98% 6.160% 4 9.631 517 522 534 rVB2 79046 280305 4.95% 0.871% 5 11.887 763 768 786 rBV 2143599 4664245 82.34% 14.496%

6 15.500 1156 1162 1181 rBV 2695564 5664871 100.00% 17.606% 7 2.0.772 1731 1737 1755 rBV 2749972 5627928 99.35% 17.491% 8 25.183 2211 2218 2230 rBV2 2186698 4983208 87.97% 15.488% 9 29.585 2694 2698 2705 rVB 66249 129486 2.29% 0.402% 10 31.712 2925 2930 2936 rBV2 28738 68631 1.21% 0.213%

11 31.804 2936 2940 2949 rVB 27984 67599 1.19% 0.210% 12 33.180 3084 3090 3112 rBV2 1517497 3509883 61.96% 10.909% 13 33.445 3114 3119 3127 rW 34720 88431 1.56% 0.275% 14 37.269 3529 3536 3556 rBV2 991503 2741659 48.40% 8.521%

Sum of corrected areas: 32175473

26624.D NP112701.M Fri Dec 07 14:47:38 2001

NYC-WTC_000031910

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NYC-WTC_000031910Source: NYC Law Department, mirrored locally

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