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GCMS comments for sample AD26532 detecting 1,1,2,2-Tetrachloroethane

Machine-extracted title · confidence 100%

Analysis report dated December 16, 2001, identifying 1,1,2,2-Tetrachloroethane at 0.80 ug/L in sample AD26532.

NYC-WTC_000031762–000031774

Folder label: “GCMS X 11/6/01 A 12/7/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

’ Data File C:\HPCHEM\1\DATA\DEC0 7 01\26532.D Vial: 8 Acq On 8 Dec 2001 12:29 am Operator: GALOS Sample gc/ms unknown 11/6 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % Of # min scan scan scan TY height area % max. total

1 5.055 19 23 33 rBV 208867 517843 6.73% 1.156% 2 7.192 251 256 266 rBV 1192431 2151898 27.97% 4.804% 3 7.852 324 328 345 rVB 1102374 2379117 30.92% 5.311% 4 9.622 516 521 535 rVB3 66332 249832 3.25% 0.558% 5 11.878 762 767 780 rBV 3000912 6268236 81.47% 13.993%

6 15.491 1155 1161 1179 rBV 3800730 7682275 99.85% 17.149% 7 17.646 1391 1396 1401 rVB2 . 41669 77444 1.01% 0.173% 8 20.764 1730 1736 1756 rBV 3827737 7693591 100.00% 17.175% 9 25.175 2209 2217 2229 rBV2 3293033 7122765 92.58% 15.900% 10 25.312 2229 2232 2246 rVB2 29416 104748 1.36% 0.234%

11 33.180 3083 3090 3108 rBV2 2570762 5713110 74.26% 12.754% 12 37.270 3528 3536 3553 rBV2 1746071 4835071 62.85% 10.794% t

Sum of corrected areas: 44795930

26532.D NP112701.M Thu Dec 13 11:23:03 2001

NYC-WTC_000031768

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NYC-WTC_000031768Source: NYC Law Department, mirrored locally

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