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GCMS analysis report for sample AD26394, Dec 2001

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DEP lab report dated December 4, 2001, documenting GCMS analysis of sample AD26394 noting other unknown compounds.

NYC-WTC_000031567–000031578

Folder label: “GCMS X 11/5/01 A 12/1/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File C:\HPCHEM\1\DATA\NOV3 0 01\263 94.D Vial: 20 Acq On 1 Dec 2001 5:29 am Operator: GALOS Sample gc/ms unknown 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 5.060 19 24 33 rVB 119196 229061 . 1.64% 0.321% 2 7.857 325 329 345 rVB 789044 1619488 11.60% 2.271% 3 10.323 591 598 605 rBV 111791 209850 1.50% 0.294% 4 10.534 617 621 630 rVB 96422 189001 1.35% 0.265% 5 11.745 749 753 759 rBV 145164 269777 1.93% 0.378% 6 11.892 763 769 790 rVB 5040666 10493539 75.14% 14.715% 7 15.495 1155 1162 1180 rBV 6018189 13965751 100.00% 19.584% 8 20.777 1730 1738 1752 rBV 6387888 13662763 97.83% 19.159% 9 25.188 2212 2219 2231 rBV2 5988518 12663061 90.67% 17.757% 10 33.194 3085 3092 3110 rBV2 4400710 9754915 69.85% 13.679% 11 37.284 3529 3538 3559 rBV2 3079802 8254307 59.10% 11.575%

Sum of corrected areas: 71311513 26394.D NP112701.M Tue Dec 04 10:44:03 2001

NYC-WTC_000031573

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NYC-WTC_000031573Source: NYC Law Department, mirrored locally

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