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GCMS analysis report for sample AD26471, Dec 2001

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DEP lab report dated December 4, 2001, documenting GCMS analysis of sample AD26471 noting other unknown compounds.

NYC-WTC_000031602–000031610

Folder label: “GCMS X 11/5/01 A 12/1/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File C: \HPCHEM\ 1 \DATA\NOV3 001\26470.D Vial: 23 Acq On 1 Dec 2001 8:12 am Operator: GALOS Sample gc/ms unknown 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 5.051 18 23 31 rVB 105721 194296 1.59% 0.316% 2 7.857 325 329 344 rBV 530340 1074847 8.81% 1.748% 3 10.314 593 597 607 rVB 70778 141358 1.16% 0.230% 4 11.745 749 753 759 rVB 127619 242545 1.99% 0.394% 5 11.882 763 768 790 rVB 4491094 9479741 77.66% 15.418% 6 15.495 1155 1162 1180 rBV 5498984 12206513 100.00% 19.853% 7 20.777 1730 1738 1757 rBV 5527463 11893170 97.43% 19.343% 8 25.188 2212 2219 2231 rBV2 4977709 10956748 89.76% 17.820% 9 33.184 3084 3091 3108 rBV2 3566135 8355008 68.45% 13.589% 10 37.274 3529 3537 3553 rBV2 2518670 6940216 56.86% 11.288%

Sum of corrected areas: 61484442 26470.D NP112701.M Tue Dec 04 15:46:34 2001

NYC-WTC_000031605

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NYC-WTC_000031605Source: NYC Law Department, mirrored locally

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