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GCMS analysis report for sample AD26434, Dec 2001

Machine-extracted title · confidence 100%

DEP lab report dated December 4, 2001, documenting GCMS analysis of sample AD26434 noting other unknown compounds.

NYC-WTC_000031592–000031601

Folder label: “GCMS X 11/5/01 A 12/1/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\NOV3001\26434.D Vial: 22 Acq On 1 Dec 2001 7:18 am Operator: GALOS Sample gc/ms unknown 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 5.055 16 23 29 rVB 122250 222269 1.76% 0.341% 2 7.861 325 329 341 rVB 741528 1544892 12.23% 2.367% 3 10.319 591 597 602 rBV 111019 200708 1.59% 0.308% 4 10.530 614 620 629 rBV 98206 185997 1.47% 0.285% 5 11.740 748 752 758 rVB 123519 244388 1.94% 0.374%

6 11.887 762 768 783 rW 4765460 9611003 76.10% 14.727% 7 15.500 1155 1162 1179 rBV 5869103 12629610 100.00% 19.353% 8 20.772 1730 1737 1758 rBV 5829979 12537361 99.27% 19.211% 9 25.183 2212 2218 2230 rBV2 5147918 11617577 91.99% 17.802% 10 33.189 3084 3091 3104 rBV2 3925912 8865415 70.20% 13.585%

11 37.279 3528 3537 3551 IBV2 2711752 7600575 60.18% 11.647%

Sum of corrected areas: 65259795 26434.D NP112701.M Tue Dec 04 15:41:36 2001

NYC-WTC_000031595

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NYC-WTC_000031595Source: NYC Law Department, mirrored locally

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