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GCMS analysis results for sample AD26711, Dec 10 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD26711 identifying unknown compounds on December 10, 2001.

NYC-WTC_000032128–000032141

Folder label: “GCMS X 11/7/01 A 12/6/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\DEC0 5 01\26711.D Vial: 5 Acq On 5 Dec 2001 12:24 pm Operator: GALOS Sample gc/ms unknown 11/7 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 5.050 20 23 34 rBV 410467 1011954 11.62% 2.067% 2 7.187 251 256 266 rBV 1705181 3110250 35.73% 6.354% 3 7.847 324 328 342 rBV 1401923 2745124 31.53% 5.608% 4 9.608 516 520 531 rVB2 65739 239955 2.76% 0.490% 5 11.873 761 767 783 rBV 3498957 7082185 81.35% 14.469%

6 15.486 1155 1161 1180 rBV 4149377 8705816 100.00% 17.786% 7. 20.758 1729 1736 1749 rBV 3961562 8536641 98.06% 17.441% 8 25.169 2210 2217 2228 rBV2 3361441 7635237 87.70% 15.599% 9 25.307 2229 2232 2245 rVB 35156 107051 1.23% 0.219% 10 33.166 3082 3089 3105 rBV2 2409503 5516204 63.36% 11.270%

11 33.431 3114 3118 3129 rVB 45159 103975 1.19% 0.212% 12 37.255 3527 3535 3553 rBV2 1508832 4152718 47.70% 8.484%

Sum of corrected areas: 48947110

26711 .D NP112701 .M Fri Dec 07 13:14:24 2001

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NYC-WTC_000032133Source: NYC Law Department, mirrored locally

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