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GCMS comments for sample AD26533 detecting 1,1,2,2-Tetrachloroethane

Machine-extracted title · confidence 95%

Analysis report dated December 16, 2001, identifying 1,1,2,2-Tetrachloroethane at 0.72 ug/L in sample AD26533.

NYC-WTC_000031788–000031800

Folder label: “GCMS X 11/6/01 A 12/7/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\DEC0701\26533.D Vial: 7 Acq On 7 Dec 2001 11:35 pm Operator: GALOS Sample gc/ms unknown 11/6 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 5.051 19 23 32 rBV 150877 382921 6.48% 1.152% 2 7.187 251 256 271 rVB 694693 1401362 23.71% 4.218% 3 7.857 325 329 347 rBV 816056 1981227 33.52% 5.963% 4 9.618 516 521 531 rBV3 48125 173071 2.93% 0.521% 5 11.883 762 768 783 rBV 2176142 4796908 81.15% 14.437%

6 15.486 1156 1161 1178 rBV 2654341 5796595 98.06% 17.446% 7 17.651 1392 1397 1401 rBV 37585 67758 1.15% 0.204% 8 20.759 1730 1736 1754 rBV 2767172 5911115 100.00% 17.790% 9 25.170 2209 2217 2230 rBV2 2423096 5303500 89.72% 15.962% 10 25.317 2230 2233 2242 rVB4 21525 65054 1.10% 0.196%

11 33.175 3083 3090 3110 rBV2 1784628 4057413 68.64% 12.211% 12 37.265 3528 3536 3552 rBV2 1139142 3289611 55.65% 9.901%

Sum of corrected areas: 33226535

26533.D NP112701.M Thu Dec 13 11:23:33 2001

NYC-WTC_000031794

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NYC-WTC_000031794Source: NYC Law Department, mirrored locally

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