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GCMS results log, sample AD27008, Dec 11 2001

Machine-extracted title · confidence 100%

Laboratory report for GCMS analysis of sample AD27008 completed on December 11, 2001.

NYC-WTC_000032520–000032533

Folder label: “GCMS X 11/8/01 A 12/7/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\DEC0 601\27008.D Vial: 21 Acq On 7 Dec 2001 4:21 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 5.041 16 22 30 rVB 111218 208172 2.20% 0.427% 2 6.591 187 191 201 rVB 61552 136318 1.44% 0.280% 3 7.857 325 329 345 rVB 623090 1263071 13.34% 2.592% 4 11.891 763 769 791 rBV 3706067 7593614 80.22% 15.586% 5 15.504 1156 1163 1179 rBV 4426470 9465840 100.00% 19.429%

6 20.777 1731 1738 1760 rBV 4515572 9340179 98.67% 19.171% 7 25.188 2212 2219 2230 rBV2 3954057 8512026 89.92% 17.471% 8 25.326 2230 2234 2243 rVB 33382 101512 1.07% 0.208% 9 29.590 2695 2699 2708 rBV2 69694 149718 1.58% 0.307% 10 31.809 2936 2941 2953 rVB 65902 165999 1.75% 0.341%

11 32.799 3043 3049 3056 rBV2 39649 110056 1.16% 0.226% 12 33.194 3085 3092 3108 rBV2 2731959 6340112 66.98% 13.013% 13 33.744 3147 3152 3163 rBV 39488 129566 1.37% 0.266% 14 37.283 3530 3538 3556 rBV2 1858639 5205112 54.99% 10.683%

Sum of corrected areas: 48721295

27008.D NP112701.M Tue Dec 11 14:57:44 2001

NYC-WTC_000032526

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NYC-WTC_000032526Source: NYC Law Department, mirrored locally

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