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GCMS results log, sample AD26845, Dec 11 2001

Machine-extracted title · confidence 100%

Laboratory report for GCMS analysis of sample AD26845 completed on December 11, 2001, indicating unknown compounds.

NYC-WTC_000032308–000032320

Folder label: “GCMS X 11/8/01 A 12/7/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

' Data File C:\HPCHEM\l\DATA\DEC0601\26845.D Vial: 29 Acq On 7 Dec 2001 12:35 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method ' : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 5.051 17 23 31 rVB 113272 209489 1.97% 0.369% 2 6.600 188 192 202 rW 54931 126069 1.18% 0.222% 3 7.857 325 329 343 rBV 665554 1342364 12.61% 2.366% 4 11.892 763 769 783 rBV 4123342 8473420 79.62% 14.936% 5 14.514 1050 1055 1061 rVB 56435 112655 1.06% 0.199%

6 15.505 1156 1163 1179 rBV 4827841 10642333 100.00% 18.759% 7 20.777 1731 1738 1758 rBV 5006342 10580705 99.42% 18.651% 8 25.188 2212 2219 2230 rBV2 4604985 9948055 93.48% 17.536% 9 25.326 2230 2234 2246 rVB2 41010 125606 1.18% 0.221% 10 29.590 2694 2699 2707 rBV2 64312 138568 1.30% 0.244%

11 31.809 2936 2941 2950 rVB 78495 185748 1.75% 0.327% 12 32.799 3044 3049 3060 rBV2 54151 156247 1.47% 0.275% 13 33.194 3084 3092 3110 rBV2 3438444 7849413 73.76% 13.836% 14 33.753 3147 3153 3165 rBV2 55147 182580 1.72% 0.322% 15 37.283 3530 3538 3558 rBV2 2424394 6657303 62.55% 11.735%

Sum of corrected areas: 56730555

26845.D NP112701.M Tue Dec 11 14:47:17 2001

NYC-WTC_000032314

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NYC-WTC_000032314Source: NYC Law Department, mirrored locally

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