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GCMS results log, sample AD26988, Dec 11 2001

Machine-extracted title · confidence 100%

Laboratory report for GCMS analysis of sample AD26988 completed on December 11, 2001.

NYC-WTC_000032448–000032461

Folder label: “GCMS X 11/8/01 A 12/7/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\DEC0601\26988.D Vial: 15 Acq On 6 Dec 2001 10:54 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Misc Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 5.044 16 22 32 rVB 110695 207798 2.29% 0.446% 2 6.594 186 191 2 00 rW 61546 138410 1.52% 0.297% 3 7.850 324 328 336 rBV 541061 1147160 12.62% 2.462% 4 11.885 763 768 788 rVB 3524924 7262824 79.87% 15.586% 5 15.498 1156 1162 1180 rBV 4357142 9092937 100.00% 19.513%

6 20.771 1731 1737 1757 rBV 4188935 8981546 98.77% 19.274% 7 25.181 2212 2218 2230 rBV2 3756999 8213886 90.33% 17.627% 8 29.592 2693 2699 2706 rBV 76823 169105 1.86% 0.363% 9 31.710 2922 2930 2935 rBV2 39866 92350 1.02% 0.198% 10 31.802 2936 2940 2952 rVB 62513 167922 1.85% 0.360%

11 32.793 3043 3048 3057 rBV 38917 114451 1.26% 0.246% 12 33.187 3085 3091 3104 rBV2 2658779 5974157 65.70% 12.820% 13 33.746 3147 3152 3161 rBV 43684 122845 1.35% 0.264% 14 37.277 3528 3537 3554 rBV2 1791341 4913889 54.04% 10.545%

Sum of corrected areas: 46599280

26988.D NP112701.M Tue Dec 11 14:53:28 2001

NYC-WTC_000032454

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NYC-WTC_000032454Source: NYC Law Department, mirrored locally

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