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GCMS comments for sample AD26710 detecting phthalate and tetrachloroethane

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Analysis report dated December 31, 2001, identifying bis(2-Ethylhexyl)phthalate and 1,1,2,2-Tetrachloroethane in sample AD26710.

NYC-WTC_000032114–000032127

Folder label: “GCMS X 11/7/01 A 12/6/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\DEC0501\26710.D Vial: 4 Acq On 5 Dec 2001 11:29 am Operator: GALOS Sample gc/ms unknown 11/7 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208,625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 5.052 19 23 34 rBV 724745 1555666 18.52% 3.120% 2 6.473 173 178 185 rBV3 28133 84702 1.01% 0.170% 3 7.188 250 256 273 rVB 2111457 4070871 48.45% 8.163% 4 7.849 324 328 345 rBV 1342550 2747505 32.70% 5.510% 5 9.362 488 493 500 rBV 70594 142274 1.69% 0.285%

6 9.609 515 520 531 rVB2 134467 468575 5.58% 0.940% 7 10.315 592 597 605 rVB 46382 96497 1.15% 0.194% 8 10.526 615 620 626 rBV 43883 90576 1.08% 0.182% 9 11.865 761 766 779 rBV 3163612 6795367 80.88% 13.627% 10 15.478 1154 1160 1180 rBV 4046210 8401347 100.00% 16.847%

11 20.751 1729 1735 1755 rBV 3951146 8269016 98.42% 16.582% 12 25.162 2210 2216 2228 rBV2 3451309 7526256 89.58% 15.092% 13 25.299 2228 2231 2240 rVB2 30626 94619 1.13% 0.190% 14 33.167 3082 3089 3109 rBV2 2400961 5469871 65.11% 10.969% 15 33.433 3114 3118 3128 rVB 43651 100012 1.19% 0.201%

16 37.248 3527 3534 3552 rBV2 1435476 3954450 47.07% 7.930%

Sum of corrected areas: 49867604

26710 .D NP112701.M Fri Dec 07 13:13:54 2001

NYC-WTC_000032119

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NYC-WTC_000032119Source: NYC Law Department, mirrored locally

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