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GCMS results log, sample AD27012, Dec 11 2001

Machine-extracted title · confidence 100%

Laboratory report for GCMS analysis of sample AD27012 completed on December 11, 2001.

NYC-WTC_000032575–000032586

Folder label: “GCMS X 11/8/01 A 12/7/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\DEC0601\27012.D Vial: 20 Acq On 7 Dec 2001 3:27 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 5.046 15 22 29 rVB 105674 206202 1.92% 0.374% 2 6.596 187 191 2 01 rW 62261 135553 1.26% 0.246% 3 7.861 325 329 346 rBV 621038 1338513 12.46% 2.426% 4 11.887 763 768 781 rBV 4133093 8572165 79.79% 15.536% 5 15.500 1156 1162 1180 rBV 5048620 10743383 100.00% 19.471%

6 20.782 1731 1738 1759 rBV 4820219 10514290 97.87% 19.056% 7 25.183 2212 2218 2230 rBV2 4334717 9681509 90.12% 17.546% 8 25.330 2230 2234 2244 rVB2 38763 110888 1.03% 0.201% 9 29.594 2694 2699 2706 rBV 65823 145690 1.36% 0.264% 10 31.804 2935 2940 2951 rVB 52623 149155 1.39% 0.270%

11 33.189 3084 3091 3112 rBV2 3255603 7346911 68.39% 13.315% 12 33.748 3146 3152 3165 rBV3 34110 120888 1.13% 0.219% 13 37.279 3529 3537 3559 rBV2 2206084 6111548 56.89% 11.076%

Sum of corrected areas: 55176695

27012.D NP112701.M Tue Dec 11 15:00:24 2001

NYC-WTC_000032581

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NYC-WTC_000032581Source: NYC Law Department, mirrored locally

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