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GCMS analysis results for sample AD26317, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD26317 with unidentified compounds detected.

NYC-WTC_000031274–000031283

Folder label: “GCMS X 11/3/01 A 12/1/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\NOV3001\26317.D Vial: 16 Acq On : 1 Dec 2001 1:51 am Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise 2 Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 5.037 15 21 28 rVB 108794 215826 1.84% 0.368% 2 5.211 37 40 46 rW 82973 137347 1.17% 0.234% 3 6.137 138 141 154 rBV 50527 122476 1.04% 0.209% 4 6.587 186 190 201 rW 68480 148231 1.26% 0.253% 5 7.852 324 328 343 rBV 962451 1938732 16.54% 3.307% 6 10.328 593 598 606 rVB 94411 188927 1.61% 0.322% 7 10.530 615 620 629 rBV 73569 151954 1.30% 0.259% 8 11.749 749 753 760 rBV 121185 235870 2.01% 0.402% 9 11.896 763 769 791 rVB 4330379 9226597 78.70% 15.740% 10 15.500 1156 1162 1179 rBV 5361780 11724188 100.00% 20.001% 11 20.782 1731 1738 1753 rBV 5200955 11189169 95.44% 19.088% 12 25.193 2212 2219 2231 rBV2 4546224 10050301 85.72% 17.145% 13 33.189 3084 3091 3105 rBV2 3329306 7376896 62.92% 12.585% 14 37.279 3529 3537 3553 rBV2 2193241 5911740 50.42% 10.085%

Sum of corrected areas: 58618254 26317.D NP112701.M Tue Dec 04 10:12:19 2001

NYC-WTC_000031279

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NYC-WTC_000031279Source: NYC Law Department, mirrored locally

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