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GCMS comments for sample AD26473 detecting N,N-dimethylbenzenesulfonamide

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DEP lab report dated December 10, 2001, identifying N,N-dimethylbenzenesulfonamide at 0.49 ug/L in sample AD26473.

NYC-WTC_000031636–000031649

Folder label: “GCMS X 11/5/01 A 12/1/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\NOV3001\26473.D Vial: 9 Acq On : 30 Nov 2001 7:30 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise 2 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 5.041 15 22 32 rVB 111106 210151 1.96% 0.363% 2 6.591 187 191 202 rW 60258 132386 1.23% 0.229% 3 7.857 325 329 344 rVB 726539 1454376 13.53% 2.514% 4 10.323 592 598 605 rBV 84659 158773 1.48% 0.274% 5 10.534 617 621 628 rVB 72469 136589 1.27% 0.236%

6 11.745 748 753760 rBV 102577 207860 1.93% 0.359% 7 11.892 763 769781 rVB 4145808 8348555 77.69% 14.432% 8 15.505 1156 1163 1180 rBV 5136117 10745620 100.00% 18.576% 9 20.777 1731 1738 1757 rBV 5047588 10443283 97.19% 18.054% 10 22.556 1927 1932 1945 rBV 1417896 2558528 23.81% 4.423% 11 23.565 2036 2042 2059 rBV 78653 229923 2.14% 0.397% 12 25.188 2213 2219 2231 rBV2 4475591 9435677 87.81% 16.312% 13 28.985 2628 2633 2645 rVB 408645 799598 7.44% 1.382% 14 30.580 2802 2807 2818 rBV 215041 427963 3.98% 0.740% 15 33.194 3084 3092 3105 rBV2 3017740 6926177 64.46% 11.974% 16 37.274 3530 3537 3549 rBV2 2020022 5630138 52.39% 9.733%

Sum of corrected areas: 57845597 26473.D NP112701.M Tue Dec 04 10:45:10 2001

NYC-WTC_000031640

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NYC-WTC_000031640Source: NYC Law Department, mirrored locally

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