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GCMS Analysis Report for Sample AD26386, Dec 2001

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Report documenting GCMS analysis of sample AD26386 with a note regarding unknown compounds.

NYC-WTC_000031415–000031432

Folder label: “GCMS X 11/5/01 A 12/1/01

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NYC 9/11 Public Portal Document LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\NOV3001\26386.D Vial: 12 Acq On : 30 Nov 2001 10:13 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Misc Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 5.013 10 19 25 rBV 261319 580103 5.10% 0.898% 2 5.095 25 28 32 rW 176972 365882 3.22% 0.566% 3 5.169 32 36 55 rVB2 276900 949598 8.35% 1.469% 4 6.104 135 138 155 rBV 144358 480759 4.23% 0.744% 5 6.462 173 177 181 rBV 58687 121320 1.07% 0.188% 6 6.572 185 189 199 rVB 61280 144868 1.27% 0.224% 7 6.700 199 203 205 rBV 60055 116042 1.02% 0.180% 8 7.186 249 256 275 rVB 2237838 4480037 39.38% 6.933% 9 7.846 324 328 335 rBV 1175734 2304207 20.25% 3.566% 10 9.360 489 493 502 rBV 66566 153166 1.35% 0.237% 11 10.322 593 598 608 rBV 347691 753211 6.62% 1.166% 12 10.533 616 621 630 rBV 191233 384399 3.38% 0.595% 13 11.744 748 753 762 rVB2 111497 244101 2.15% 0.378% 14 11.891 763 769 780 rBV 4381254 8921271 78 .41% 13.806% 15 15.504 1157 1163 1182 rBV 5558460 11377570 100.00% 17.607% 16 20.776 1732 1738 1757 rBV 5160487 10908346 95.88% 16.881% 17 25.187 2212 2219 2231 rBV2 4513965 9755200 85.74% 15.096% 18 33.193 3085 3092 3106 rBV2 3135759 7056194 62.02% 10.919% 19 37.282 3530 3538 3555 rBV2 2041985 5524709 48.56% 8.549%

Sum of corrected areas: 64620983 26386.D NP112701.M Tue Dec 04 10:38:29 2001

NYC-WTC_000031421

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NYC-WTC_000031421Source: NYC Law Department, mirrored locally

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