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GCMS analysis report for sample AD26393, Dec 2001

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DEP lab report dated December 4, 2001, documenting GCMS analysis of sample AD26393 noting other unknown compounds.

NYC-WTC_000031550–000031566

Folder label: “GCMS X 11/5/01 A 12/1/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\NOV3001\26393.D Vial: 3 Acq On : 30 Nov 2001 2:02 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 5.009 9 18 27 rBV2 112680 446699 4.02% 0.722% 2 5.119 27 30 34 rW 258402 461842 4.16% 0.746% 3 5.183 34 37 54 rVB 378263 955844 8.61% 1.545% 4 5.669 86 90 104 rVB 60084 162962 1.47% 0.263% 5 6.118 135 139 154 rBV 221095 560784 5.05% 0.906% 6 6.467 173 177 186 rBV 66940 156476 1.41% 0.253% 7 6.577 186 189 193 rBV 66172 113419 1.02% 0.183% 8 6.705 200 203 212 rBV2 57771 149664 1.35% 0.242% 9 7.182 248 255 268 rBV 1472567 3177827 28.63% 5.135% 10 7.842 324 327 335 rBV 999231 2103690 18.95% 3.400% 11 10.327 592 598 607 IBV 363899 802808 7.23% 1.297% 12 10.529 616 620 630 rBV 175243 362022 3.26% 0.585% 13 11.749 748 753 761 rBV 109129 232174 2.09% 0.375% 14 11.886 763 768 779 rVB 4189538 8654066 77.97% 13.985% 15 15.499 1156 1162 1179 rBV 5279297 11099516 100.00% 17.937% 16 20.772 1731 1737 1755 rBV 4938525 10636492 95.83% 17.188% 17 25.183 2211 2218 2231 rBV2 4331454 9513833 85.71% 15.374% 18 33.188 3084 3091 3107 rBV2 3088554 6864128 61.84% 11.092% 19 37.278 3529 3537 3549 rBV2 1991319 5427583 48.90% 8.771%

Sum of corrected areas: 61881829 26393.D NP112701.M Tue Dec 04 10:43:43 2001

NYC-WTC_000031555

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NYC-WTC_000031555Source: NYC Law Department, mirrored locally

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