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GCMS Analysis Report for Sample AD26389, Dec 2001

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Report documenting GCMS analysis of sample AD26389 with a note regarding unknown compounds.

NYC-WTC_000031473–000031490

Folder label: “GCMS X 11/5/01 A 12/1/01

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NYC 9/11 Public Portal Document LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\NOV3001\26389.D Vial: 6 Acq On : 30 Nov 2001 4:46 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC

peak R.T. first max last PK peak peak peak % Of # min scan scan scan TY height area % max. total 1 4.977 5 15 19 rBV 30994 167333 1.53% 0.282% 2 5.041 19 22 31 rW2 77354 208839 1.91% 0.351% 3 5.151 31 34 38 rW 273132 445903 4.08% 0.750% 4 5.216 38 41 54 rVB 380409 741706 6.79% 1.248% 5 5.692 89 93 102 rVB 61551 130502 1.19% 0.220% 6 6.142 138 142 155 rVB 236370 502028 4.60% 0.845% 7 6.490 175 180 187 rBV 57784 123265 1.13% 0.207% 8 6.591 187 191 201 rVB 65229 140686 1.29% 0.237% 9 6.719 201 205 213 rBV2 50085 119134 1.09% 0.200% 10 7.187 248 256 266 rBV 785232 1887330 17.28% 3.175% 11 7.857 325 329 342 rBV 741237 1497545 13.71% 2.519% 12 10.323 593 598 608 rBV 347601 656622 6.01% 1.105% 13 10.534 616 621 629 rBV 150237 285903 2.62% 0.481% 14 11.745 749 753 761 rBV 113503 229246 2.10% 0.386% 15 11.891 763 769 781 rVB 4243968 8505172 77.86% 14.309% 16 15.504 1156 1163 1180 rBV 5094031 10923701 100.00% 18.377% 17 20.777 1731 1738 1758 rBV 5102113 10635949 97.37% 17.893% 18 25.188 2212 2219 2230 rBV2 4463894 9541093 87.34% 16.051% 19 33.194 3084 3092 3104 rBV2 3103934 7035184 64.40% 11.836% 20 37.274 3529 3537 3552 rBV2 2077700 5663516 51.85% 9.528%

Sum of corrected areas: 59440657 26389.D NP112701.M Tue Dec 04 10:41:00 2001

NYC-WTC_000031479

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