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GCMS analysis report for sample AD26474, Dec 2001

Machine-extracted title · confidence 100%

DEP lab report dated December 4, 2001, documenting GCMS analysis of sample AD26474 noting other unknown compounds.

NYC-WTC_000031650–000031660

Folder label: “GCMS X 11/5/01 A 12/1/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\NOV3001\26474.D Vial: 8 Acq On : 30 Nov 2001 6:35 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise ! Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 5.050 18 23 32 rVB 121697 247631 1.96% 0.389% 2 5.234 40 43 48 rW 79450 130950 1.03% 0.206% 3 6.600 187 192 202 rW 72931 156699 1.24% 0.246% 4 7.856 325 329 342 rBV 919307 1861713 14.71% 2.925% 5 10.323 593 598 606 rBV 115219 206226 1.63% 0.324%

6 10.534 616 621 628 rBV 91974 175152 1.38% 0.275% 7 11.744 748 753 760 rBV 126855 252557 2.00% 0.397% 8 11.891 763 769 783 rVB 4817981 9752666 77.04% 15.324% 9 15.504 1156 1163 1179 rBV 5733346 12658773 100.00% 19.890% 10 20.777 1731 1738 1755 rBV 5808100 12269832 96.93% 19.279%

11 25.188 2212 2219 2232 rBV2 5150273 11068985 87.44% 17.392% 12 33.193 3085 3092 3105 rBV2 3557438 8167015 64.52% 12.832% 13 37.283 3529 3538 3549 rBV2 2479645 6695898 52.90% 10.521%

Sum of corrected areas: 63644097

26474.D NP112701.M Tue Dec 04 10:45:31 2001

NYC-WTC_000031654

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NYC-WTC_000031654Source: NYC Law Department, mirrored locally

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