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GCMS analysis report for sample AD26472, Dec 2001

Machine-extracted title · confidence 100%

DEP lab report dated December 4, 2001, documenting GCMS analysis of sample AD26472 noting other unknown compounds.

NYC-WTC_000031611–000031623

Folder label: “GCMS X 11/5/01 A 12/1/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\NOV3001\26471.D Vial: 11 Acq On : 30 Nov 2001 9:19 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table " Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % Of # min scan scan scan TY height area % max. total

1 5.046 17 22 32 rVB 108996 216658 1.79% 0.346% 2 7.861 325 329 343 rVB 823575 1653561 13.67% 2.641% 3 10.328 591 598 604 rBV 99923 193033 1.60% 0.308% 4 10.530 615 620 627 rBV 88306 169714 1.40% 0.271% 5 11.749 748 753 759 rBV 122872 235757 1.95% 0.376%

6 11.887 763 768 781 rW 4488213 9279332 76.72% 14.819% 7 15.500 1156 1162 1179 rBV 5529722 12095169 100.00% 19.316% 8 20.782 1731 1738 1755 rBV 5520563 11835982 97.86% 18.902% 9 25.193 2212 2219 2231 rBV2 4994509 10917474 90.26% 17.435% 10 33.189 3084 3091 3106 rBV2 3845889 8655381 71.56% 13.822%

11 37.288 3529 3538 3549 rBV2 2619278 7366305 60.90% 11.764%

Sum of corrected areas: 62618366

26471.D NP112701.M Tue Dec 04 10:44:23 2001

NYC-WTC_000031617

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NYC-WTC_000031617Source: NYC Law Department, mirrored locally

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