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GCMS Analysis Report for Sample AD26336, Dec 2001

Machine-extracted title · confidence 100%

Report documenting GCMS analysis of sample AD26336 with a note regarding unknown compounds.

NYC-WTC_000031384–000031399

Folder label: “GCMS X 11/5/01 A 12/1/01

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NYC 9/11 Public Portal Document LSC Area Percent Report Data File C:\HPCHEM\1\DATA\NOV3001\26336 .D Vial: 30 Acq On 1 Dec 2001 2:36 pm Operator: GALOS Sample gc/ms unknown 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 4.958 8 13 16 rBV 86884 152004 1.92% 0.366% 2 5.013 16 19 25 rW 110171 197601 2.50% 0.476% 3 5.096' 25 28 33 rW 36999 98675 1.25% 0.238% 4 5.169 33 36 57 rVB 61259 271471 3.43% 0.654% 5 6.563 184 188 198 rW 51048 120341 1.52% 0.290% 6 7.168 249 254 266 rBV 370636 666837 8.43% 1.605% 7 7.838 323 327 345 rBV 943211 1998948 25.28% 4.812% 8 10.323 592 598 607 rBV 125257 250827 3.17% 0.604% 9 10.534 616 621 628 rBV 105742 211080 2.67% 0.508% 10 11.891 763 769 780 rBV 2954188 6398367 80.93% 15.404%

11 15.504 1157 1163 1181 rBV 3832554 7906033 100.00% 19.033% 12 20.777 1731 1738 1755 rBV 3671392 7854338 99.35% 18.909% 13 25.187 2212 2219 2230 rBV2 3020360 6946132 87.86% 16.723% 14 25.325 2230 2234 2243 rVB2 29020 86382 1.09% 0.208% 15 33.184 3084 3091 3104 rBV2 2151240 4638314 58.67% 11.167% 16 37.273 3529 3537 3549 rBV2 1417136 3740275 47.31% 9.005%

Sum of corrected areas: 41537625 26336.D NP112701.M Tue Dec 04 15:07:45 2001

NYC-WTC_000031390

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NYC-WTC_000031390Source: NYC Law Department, mirrored locally

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