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GCMS analysis results for sample AD26315, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD26315 with unidentified compounds detected.

NYC-WTC_000031248–000031261

Folder label: “GCMS X 11/3/01 A 12/1/01

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NYC 9/11 Public Portal Document LSC Area Percent Report Data File C:\HPCHEM\1\DATA\NOV3001\26315.D Vial: 24 Acq On 1 Dec 2001 9:07 am Operator: GALOS Sample gc/ms unknown 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak peak peak % Of # min scan scan scan TY height area % max. total

1 5.031 15 21 30 rVB 116493 235001 3.28% 0.610% 2 5.151) 30 34 37 rBV 60283 109154 1.52% 0.283% 3 5.206 37 40 46 rW 78906 140764 1.96% 0.366% 4 6.132 137 141 147 rBV 49164 106119 1.48% 0.276% 5 6.581 186 190 194 rBV 45524 88676 1.24% 0.230%

6 7.177 249 255 262 rBV 48117 98748 1.38% 0.256% 7 7.847 324 328 341 rBV 807337 1666798 23.25% 4.329% 8 10.313) 592 597 606 rBV 101817 199982 2.79% 0.519% 9 10.524/ 616 620 629 rVB 79454 156106 2.18% 0.405% 10 11.881 763 768 782 rVB 2645350 5633745 78.58% 14.631%

11 15.495 1156 1162 1180 rBV 3452260 7133400 99.49% 18.526% 12 20.767 1731 1737 1749 rBV 3396444 7169673 100.00% 18.620% 13 25.178 2212 2218 2230 IBV2 3104585 6697495 93.41% 17.394% 14 25.316 2230 2233 2242 rVB 28615 72718 1.01% 0.189% 15 33.184 3085 3091 3106 rVB2 2285850 4904497 68.41% 12.738% 16 37.264 3529 3536 3548 rBV2 1501073 4091419 57.07% 10.626%

Sum of corrected areas: 38504295 26315.D NP112701.M Tue Dec 04 10:11:41 2001

NYC-WTC_000031254

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NYC-WTC_000031254Source: NYC Law Department, mirrored locally

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