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GCMS Analysis Report for Sample AD26337, Dec 2001

Machine-extracted title · confidence 100%

Report documenting GCMS analysis of sample AD26337 detecting unknown compounds and DDD.

NYC-WTC_000031400–000031414

Folder label: “GCMS X 11/5/01 A 12/1/01

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NYC 9/11 Public Portal Document LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\NOV3001\26337.D Vial: 25 Acq On 1 Dec 2001 10:01 am Operator: GALOS Sample gc/ms unknown 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 4.928 6 9 14 rW 53125 97408 1.46% 0.279% 2 5.001 14 17 24 rW 101.141 192533 2.89% 0.551% 3 5.093 24 27 30 rW 26567 68900 1.03% 0.197% 4 5.157 31 34 58 rVB2 46857 294963 4.42% 0.844% 5 6.101 132 137 143 rBV 19488 68050 1.02% 0.195%

6 6.560 182 187 197 rW 41648 105317 1.58% 0.301% 7 7.165 248 253 271 rVB 292494 609967 9.15% 1.745% 8 7.835 323 326 346 rVB 657656 1542969 23.15% 4.414% 9 10.320 593 597 603 rBV 102907 210827 3.16% 0.603% 10 10.531 616 620 629 rBV 89532 175158 2.63% 0.501%,

11 11.888 762 768 779 rBV 2522671 5342998 80.15% 15.286% 12 15.501 1156 1162 1181 rBV 3199791 6665951 100.00% 19.070% 13 20.774 1731 1737 1753 rBV 3172326 6618093 99.28% 18.934% 14 25.184 2211 2218 2229 rBV2 2573552 5826567 87.41% 16.669% 15 25.322 2229 2233 2242 rVB 24632 71599 1.07% 0.205%

16 33.181 3084 3090 3104 rBV2 1737881 3896178 58.45% 11.146% 17 37.271 3528 3536 3547 rBV2 1188313 3166837 47.51% 9.060%

Sum of corrected areas: 34954315

26337.D NP112701.M Fri Dec 21 14:28:40 2001

NYC-WTC_000031406

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NYC-WTC_000031406Source: NYC Law Department, mirrored locally

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