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GCMS analysis results for sample AD26681, Dec 10 2001

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Laboratory report documenting GCMS analysis of sample AD26681 identifying unknown compounds on December 10, 2001.

NYC-WTC_000032079–000032092

Folder label: “GCMS X 11/7/01 A 12/6/01

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Scanned page image, NYC-WTC_000032082
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\DEC0401\26681.D Vial: 2 Acq On 4 Dec 2001 11:44 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 4.982 12 15 21 rW 242963 461904 4.45% 0.828% 2 5.065 21 24 28 rW 114419 256098 2.47% 0.459% 3 5.129 28 31 57 rVB2 179846 773200 7.44% 1.386% 4 6.074 130 134 151 rBV 91211 341598 3.29% 0.612% 5 6.431 169 173 182 rBV 43658 121835 1.17% 0.218%

6 6.541 182 185 195 rW 47269 114034 1.10% 0.204% 7 6.670 195 199 208 rW2 39381 118279 1.14% 0.212% 8 7.146 246 251 268 rBV 695806 1373007 13.22% 2.461% 9 7.816 320 324 343 rBV •981661 2118468 20.40% 3.797% 10 10.301 590 595 604 rBV 132913 287135 2.76% 0.515%

11 10.512 613 618 627 rBV 66550 141044 1.36% 0.253% 12 11.869 760 766 780 rBV 4016119 8460660 81.46% 15.166% 13 15.482 1154 1160 1178 rBV 5157319 10386638 100.00% 18.618% 14 20.755 1729 1735 1756 rBV 4958651 10131302 97.54% 18.160% 15 25.166 2209 2216 2228 rBV2 4214871 9126016 87.86% 16.358%

16 25.303 2228 2231 2242 rVB 37728 105186 1.01% 0.189% 17 33.171 3082 3089 3106 rBV2 2898405 6481746 62.40% 11.618% 18 33.428 3111 3117 3128 rVB 60551 143631 1.38% 0.257% 19 37.252 3527 3534 3546 rBV2 1797764 4846538 46.66% 8.687%

Sum of corrected areas: 55788319

26681.D NP112701.M Fri Dec 07 13:12:15 2001

NYC-WTC_000032082

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NYC-WTC_000032082Source: NYC Law Department, mirrored locally

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