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GCMS analysis results sample AD26832, December 2001

Machine-extracted title · confidence 70%

Gas chromatography-mass spectrometry analysis of sample AD26832 documenting unknown compounds with reference to comments.

NYC-WTC_000032245–000032265

Folder label: “GCMS X 11/7/01 A 12/6/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\DEC0601\26832.D Vial: 5 Acq On 6 Dec 2001 1:50 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 5.011 11 18 26 rBV3 95419 367622 5.23% 0.897% 2 5.112 26 29 • 33 rW 211696 388128 5.52% 0.947% 3 5.176 33 36 56 rVB 321893 904175 12.86% 2.206% 4 5.662 86 89 98 rVB 48751 108693 1.55% 0.265% 5 6.111 135 138 155 rBV 175623 506652 7.20% 1.236%

6 6.469 172 177 185 rBV 59679 149557 2.13% 0.365% 7 6.579 185 189 199 rVB 58201 147841 2.10% 0.361% 8 6.698 199 202 211 rBV 55296 133633 1.90% 0.326% 9 6.817 211 215 220 rBV2 39771 82267 1.17% 0.201% 10 7.175 248 254 272 rVB 798710 1742503 24.78% 4.251%

11 7.844 323 327 345 rBV 1036411 2196982 31.24% 5.360% 12 10.320 592 597 605 rBV 275533 577890 8.22% 1.410% 13 10.531 615 620 631 rBV 121463 257776 3.67% 0.629% 14 11.888 763 768 790 rVB 2783691 5759999 81.91% 14.051% 15 15.501 1156 1162 1181 rBV 3451908 7032102 100.00% 17.155%

16 20.774 1731 1737 1752 rBV 3285381 6795515 96.64% 16.578% 17 25.185 2211 2218 2230 rBV2 2847450 6160058 87.60% 15.027% 18 33.181 3084 3090 3104 rBV2 1868921 4306213 61.24% 10.505% 19 33.447 3115 3119 3127 rVB 31763 74302 1.06% 0.181% 20 37.271 3529 3536 3548 rBV2 1234067 3300386 46.93% 8.051%

Sum of corrected areas: 40992294

26832 .D NP112701.M Fri Dec 07 14:55:20 2001

NYC-WTC_000032251

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NYC-WTC_000032251Source: NYC Law Department, mirrored locally

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