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GCMS analysis results for sample AD26676, Dec 10 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD26676 identifying unknown compounds on December 10, 2001.

NYC-WTC_000031968–000031988

Folder label: “GCMS X 11/7/01 A 12/6/01

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Scanned page image, NYC-WTC_000031974
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\DEC0 6 01\26676.D Vial: 9 Acq On 6 Dec 2001 5:28 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 5.005 12 18 27 rBV 123388 438200 5.75% 0.975% 2 5.115 27 30 34 rW 210687 392402 5.15% 0.873% 3 5.179 34 37 55 rVB 310749 839262 11.01% 1.866% 4 5.665 86 90 95 rVB 40025 83207 1.09% 0.185% 5 6.115 135 139 156 rBV 182231 495781 6.50% 1.103%

6 6.463 174 177 186 rBV 58968 142481 1.87% 0.317% 7 6.573 186 189 200 rVB 68473 151416 1.99% 0.337% 8 6.701 200 203 211 rBV 60747 138267 1.81% 0.307% 9 6.821 212 216 220 rBV2 42997 79887 1.05% 0.178% 10 7.169 248 254 278 rVB 977976 1963120 25.75% 4.366%

11 7.839 323 327 334 rBV 1249675 2482114 32.56% 5.520% 12 10.314 593 597 609 rBV 243912 548910 7.20% 1.221% 13 10.525 616 620 628 rBV 121136 253594 3.33% 0.564% 14 11.883 763 768 782 rBV 2870032 6192722 81.23% 13.772% 15 15.496 1156 1162 1181 rBV 3611082 7624112 100.00% 16.955%

16 20.768 1731 1737 1755 rBV 3584557 7583398 99.47% 16.865% 17 25.179 2212 2218 2230 rBV2 3122134 6846138 89.80% 15.225% 18 25.326 2230 2234 2243 rVB2 27329 81024 1.06% 0.180% 19 33.185 3084 3091 3109 rBV2 2128609 4816467 63.17% 10.711% 20 33.451 3116 3120 3130 rVB 38487 90668 1.19% 0.202%

21 37.274 3529 3537 3550 rBV 1406787 3722299 48.82% 8.278%

Sum of corrected areas: 44965469

26676.D NP112701.M Fri Dec 07 14:51:16 2001

NYC-WTC_000031974

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NYC-WTC_000031974Source: NYC Law Department, mirrored locally

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