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GCMS analysis results for sample AD27628, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD27628 for unknown compounds and surrogates on January 3, 2002.

NYC-WTC_000033159–000033176

Folder label: “GCMS X 11/16/01 A 12/18 - 12/20/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC19O1\27628.D Vial: 18 Acq On : 20 Dec 2001 1:24 pm Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Hexanone Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

6.55 2.21 ng/uL 520856 1,4-Dichlorobenzene-d4 11.87

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexan e 100 C6H120 000591-78-6 91 2 2-Hex. .one 100 C6H120 000591-78-6 91 3 2-He: none 100 C6H120 000591-78-6 91 4 2-H, anone 100 C6H120 000591-78-6 91 Abundance Scan 186 (6.546 min): 27628.D (-) m/ z 43.1.0 100.00% 43 58 5000-

71 85 100 6.20 6.40 6.60 6.80 384 I''111'1 ‘11 53 | 1— mTTTTT 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 m/z 58.10 51.95% miz-> Abundance #1556: 2-Hexanone 43

58 IIn 5000 6.20 6.40 6.60 6.80 m/z 57 10 14.83% 27 39 100 71 85 I I J'"‘f + —hr - mm miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63385:2-Hexanone 43 — .1 r 6.20 6.40 6.60 6.80 5000- 58 m/ z 41.10 13.84% 29 39 100 .1 I .... I IM J II I TPPTT 7,1 1W99BBB 85 ——Ba)r I1”'I I. * I • I" " I'" 11'" ’ I m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63386:2-Hexanone 43 6.20 6.401 6.60 6.80 m/z 100..15 8.49% 5000- 58 29

mTTT ■ ■ r " ■ i' 71 TTT 85 ... 1' + 100 11 u ' I —.... L....— m/z 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.20 6.40 6.60 6.80

27628.D NP112701.M Fri Dec 21 09:19:14 2001 Page 4

NYC-WTC_000033170

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NYC-WTC_000033170Source: NYC Law Department, mirrored locally

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