GCMS analysis results for sample AD27954, Jan 2002

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Data File : C:\HPCHEM\1\DATA\DEC1901\27954.D Vial: 10 Acq On : 21 Dec 2001 12:22 am Operator: GALOS Sample : gems unknown 11/20 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

6.46 0.66 ng/uL 213349 1,4-Dichlorobenzene-d4 11.86

Hit# of 5 / Tentative ID MW MolForm CAS# Qual

1 3-Hexa: ne 100 C6H12O 000589-38-8 91 2 3-Hex? one 100 C6H120 000589-38-8 90 3 3-He: .none 100 C6H120 000589-38-8 78 4 3-» anone 100 C6H120 000589-38-8 72 Abundance Scan 177 (6.463 min): 27954.D (-) m/z 43.10 100.00% 43 57 71 5000 100 ‘ 1 I 11 6.20 _A 6.40 A -i 6.60 6.80

miz-> I'''' I' " ' I 34, mH । n ।'1111 85 Pguv | I « f I | I I I 4 | t I I f " " I" " P m/z !57.10 93.30% 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63358: 3-Hexanone 43

_W 57

71 TTHTf 5000 TfTr 6.20> 6.40 6.60 6.80 100 m/z 71.0,5 56.84% 85 T T I'1" I' "' I tmm "I.............. 1, rn 11" > 11111 j । T T’ miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1528: 3-Hexanone 43 57 A. AA6.20 6.40 6.60 6.80 5000 29 71 m/z 100.15 30.75% 100 85 m/z-> mmm . ।।|।।111 ■ 1111111 < । " " I " " I' 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 111 ■ । ■ 1111

Abundance #63356: 3-Hexanone 29 43 57 6.20 6.40 6.60 6.80 m/z 41.10 27.25% 5000 71

100 _ _ .. ,.38, [| ....... " ..... | > I ' I | ... I | . I . I | I I I . ....... | . I I . | ...... | |I I ...... | | 85....... t .. I I | I I I I | ..... | I | | I |< m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.20

27954.D NP112701.M Fri Dec 21 09:59:15 2001 Page 1

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