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GCMS analysis results for sample AD27679, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD27679 for unknown compounds and surrogates on January 3, 2002.

NYC-WTC_000033263–000033284

Folder label: “GCMS X 11/16/01 A 12/18 - 12/20/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1901\27679.D Vial: 6 Acq On : 19 Dec 2001 11:43 am Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Oxirane, 2-methyl-3-propyl-, c Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T.

5.66 0.56 ng/uL 124119 1,4-Dichlorobenzene-d4 11.85

Hit# of 5 Tentative ID MW. MolForm CAS# Qual

1 Oxirane, 2 -mi hyl-3-propyl-, cis- 100 C6H120 006124-90-9 74 2 Oxirane, 2-mlethyl-3-propyl- , trans- 100 C6H120 006124-91-0 32 3 Heptane, ,3-dimethyl- 128 C9H20 003074-71-3 12 4 2-Hydro/y-3-hexanone 116 C6H1202 054073-43-7 9 Abundance Scan 90 (5.665 min): 27679.D (-) m/z 41.10 100.00% 41

85 5000 57 71 ....A...... A TIP-m—mmn 5.40 5.60 5.80 6.00 1' 1 i 1 1 i miz- > Abundance ' i ' TrLI.T 20 30 40 50 60 ■ i ' ■ ' ■ i 1 70 80 90 100 #1531: Oxirane, 2-methyl-3-propyl-, cis- 110 120 130 m/ z 43.10 89.85%

43

57 —.............. - 5000 71 85 5.40 5.60 5.80 6.00 m/z 45.10 80.11% — 100 m/z-> 20 ............. 30 40 N 50 60 70 80 90 100 110 120 130 Abundance #1532: Oxirane, 2-rnetliyl-3-prapyl-. trans- 41

5.401 -A 5.60 5.80 6.00 5000 57 71 m/ z l85.05 52.73% I 85 i ’I1 iI ■ i ' 1 ■ 1 i ' ' ' ' i 1 j ............................. 100.......................................

... —LA.... ... ' ' i ‘ m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #65133: Heptane, 2,3-dimethyl- 43 5.40 5.60 5.80 6.00 m/z 57.10 45.36% 5000- 84

m/z—> 20 27 ; '] • • »' I ■ ' ' • J l 30 40 I ,. ,-.-.1,, 50 57

60 - 71

70 80 ........................................... 128 90 100 110 120 130 5.40 .. A... A 5.60 5.80 6.00

27679.D NP112701.M Thu Dec 20 11:42:06 2001 Page 3

NYC-WTC_000033273

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