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GCMS analysis results for sample AD26677, Dec 10 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD26677 identifying unknown compounds on December 10, 2001.

NYC-WTC_000031989–000032006

Folder label: “GCMS X 11/7/01 A 12/6/01

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Scanned page image, NYC-WTC_000032001
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26677.D Vial: 11 Acq On 6 Dec 2001 7:17 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 6 2,3-Butanediol Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

7.16 4.89 ng/uL 1372780 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2,3-Butanediol 90 C4H10O2 000513-85-9 28 2 N-Ethyl formamide 73 C3H7NO 000627-45-2 9 3 Isopropyl Alcohol 60 C3H80 000067-63-0 9 4 2-Butanol, 3-methyl- 88 C5H120 000598-75-4 9 Abundance Scan 253 (7.165 min): 26677.D (-) m/ z 45.05 100.00% 45

5000 - 61 73 P —

m/z-> + AH8 TTTTTTTTTTT 207 I'1 ‘1111111 ‘ ' > ‘T" '11 T"IIT 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 6.80 m/ z 7.00 43.00 7.20 7.40 76.95% 7.60

Abundance #917:2.3-Butanediol ’ 45

5000 Trrr TTI 1 2s 6.80 7.00 7.20 7.40 7.60 29 m/ z 61.00 34.65% 19 1.. , .i |H> . | 75 90 TTTTTTTTTI" ...jl .1 57 TTT I • • • ■ I' ‘ ' I'1'' I''' ’ I' *' ’ I m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 'Abundance #292: N-Ethylformaride I i 30 73 -_ — i 6.80 7.00 7.20 7.40 7.60 5000 m/ z 73.05 32.99% 44 58

15 1;____________________________________ i TTTTTT i" • ■ i111 ’ i''" i"1 -1" " i"1' i"111" " i1111111 •11"111 •1' • i" " i" " i111' i11" i" " i" ’1 r11 m/z-? 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200210 'Abundance #62359: Isopropyl Alcohol 4......... 4.......... i 45 6.80 7.00 7.20 7.40 7.60 m/ z 44.05 16.18% 5000 -

27 I

" r " ■ i" m r 59 TIUTTe T TpTep ' ’ ......................... TTTrTr TT ।1 m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 210 6.80 7.00 7.20 7.40 7.60

26677.D NP112701.M Fri Dec 07 14:52:29 2001 Page 6

NYC-WTC_000032001

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NYC-WTC_000032001Source: NYC Law Department, mirrored locally

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