GCMS analysis results for sample AD28168, Jan 2002

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Library Search Compound Report

Data File : C: \HPCHEM\ 1 \DATA\DEC2 10128164.D vial: 14 Acq On : 22 Dec 2001 5:46 am Operator: GALOS Sample : gems unknown 11/23 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 3-Hexanone Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

6.40 0.53 ng/uL 153338 1,4-Dichlorobenzene-d4 11.79

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanone 100 C6H120 000589-38-8 91 2 3-Hexanone 100 C6H120 000589-38-8 87 3 3-Hexanone 100 C6H120 000589-38-8 72 4 3-Hexanone 100 C6H120 _________ 000589-38-8 59 Abundance Scan 170 (6.404 min): 28164.D (-) m/z 43.10 . 100.00% 43 57 71 5000 100 । । A , A ।- 6.00 6.20 6.40 6.60 6.80 mmmmmm + ..............I' ..... ......... .. 1' I'''' I''' • I TTT1ITTT |TTT-IT T~TTTT ‘T rpn Trrq-rrrrj- m/z 57.10 86.37% miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1528: 3-Hexanone 43 57

29 71 5000 6.00 6.20 6.40 6.60 6.80 100 m/z 71.05 57.21%

miz- ..... r TTTTT n TIH ■'I...... 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 ....... 85..... . ""I.. Abundance #63358: 3-Hexanone 43 57 4 .....6.40 —6.20 6.00 6.60 6.80 71 m/z 100.15 5000 28.65% 100 I ......................... jj 85_______ 1‘,0u11000—TE70"TTT"TTIT"TT 11 r "11"' * IH i" " i111 111 ■ 11 > ■ ■ ■ 11 ■ H 111 ■ 1111 ■ ■ I ■" ' I m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63356:3-Hexanone 29 43 57 6.00 6.20 6.40 6.60 6.80 m/z 41.10 27.76% 5000 71

miz-> _ T ........ 38 4 ............... ............... .............. 85............... _ 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 100 AMW 6.00 6.20 6.40 6.60 6.80

28164.D NP112701.M Fri Dec 28 09:56:19 2001 Page 1

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