GCMS unknowns analysis results for sample AD27873, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1901\27873.D Vial: 5 Acq On : 20 Dec 2001 7:48 pm Operator: GALOS Sample : gems unknown 11/20 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 3-Hexanone Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

6.47 0.63 ng/uL 255173 1,4-Dichlorobenzene-d4 11.86

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanone 100 C6H120 000589-38-8 91 2 3-Hexanone 100 C6H120 000589-38-8 87 3 3-Hexanone 100 C6H120 000589-38-8 86 4 3-Hexanone 100 C6H120 000589-38-8 59 ■Abundance Scan 178 (6.473 min): 27873.D (-) m/z 43.10 . 100.00% 43 57

71 5000

39 100 • l • • • » l> — MAA, 85 6.20 6.40 6.60 6.80 mmmmm 4 HH 53 * *" r111 r TIT 11 ‘ ‘11 11 m/z 57. 10 95.02? m/z~> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63358:3-Hexanone i 4)3

5000 57

71

100 —T Tr 1r

m/z 6.20 6.40 71.05 IA_ , 6.60 6.80 53.88

miz- 'I'......... Th H . > j । n > p m|rrnpi j ‘I • 11" “ I' 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 +.. 85.— . Abundance

29 43 #63357:3-Hexanone

57 A.. ' ' ' 6.20 ' ' 6.40 ' ' 6.60 6.80 5000 71 m/z 41.10 28.74%

100

m/z-> Abundance _________________________________________ ________ 85__________________ " ' I " 1' 111 u I'1'' I' " ' I ‘ H " I " " I ’11' i " H l u 1 ‘ 1 1" I' " 11 " '<!■■" 111 nj 111111111111 < 111 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 43 #1528: 3-Hexanone 57 T 174444 6.20 m/z 100 Awl 6.40 6.60 6.80 28.60% 5000 29 71 •15 100

_ I.................1 _________ ____________4_________ ____________ .________ , \..... "‘‘I‘ITTU“TVCCIIUOOIICTTTOTTuTOTET‘uOTTTOOOOTTIWTWTTOTTTTT[ miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.20 6.40 6.60 6.80

27873.D NP112701.M Fri Dec 21 09:57:21 2001 Page 1

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