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GCMS analysis results for sample AD27632, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD27632 for unknown compounds and surrogates on January 3, 2002.

NYC-WTC_000033191–000033205

Folder label: “GCMS X 11/16/01 A 12/18 - 12/20/01

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Scanned page image, NYC-WTC_000033199
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1901\27632.D Vial: 20 Acq On : 20 Dec 2001 3:14 pm Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 3-Hexanone Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

6.48 1.01 ng/uL 273032 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanone 100 C6H120 000589-38-8 91 2 3-Hexanone 100 C6H120 000589-38-8 91 3 3-Hexanone 100 C6H120 000589-38-8 91 4 3-Hexanone 100 C6H120 000589-38-8 78 Abundance Scan 178 (6.476 min): 27632.D (-) m/z 43.10 100.00% 43 57

5000-

In 111 39 ..... 4 . ...53,H TTTrrrr ITT T T +85 71

100

■11 ■ ■" r TPTT

m/ z 6.20 s 6.40 57.10 6.60 6.80 88.90% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63358:3-Hexanone 43

5000 57

71

100 "rrrrur TTT I' ‘ m/ z 6.20 I 6.40 71.0.5 ' I • 1 • ' I "" 6.60 6.80 54.48% 85 1 > l ■ • ■ ■ l ■ ■ ■ ■ I 111—00 " I'' " I' m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 30 85 90 95 100 105 Abundance

29 43 #63357: 3-Hexanone 57 6.20 M 6.40 6.60 6.80 5000 71 m/z 100.15 29.34% 100 ___________ .__________ 85___________ | TTITTTTTTT 11"' I" " I" Tp-rrrp-rrr-p- ■i TTTn’1—TTOOTTTTTT"“T’IATP m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1528: 3-Hexanone — 4........... 43 57 6.20 6.40 6.60 6.80. m/Z 41.10 28.20% 29 71 5000 100

TTTTTTT i" " i " " I " ■ I ........... 'I' TI—Bur, H mpmm) m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.20 6.40 6.60 6.80

27632.D NP112701.M Fri Dec 21 09:20:24 2001 Page 1

NYC-WTC_000033199

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NYC-WTC_000033199Source: NYC Law Department, mirrored locally

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