GCMS unknowns analysis results for sample AD27951, Jan 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1901\27951.D Vial: 7 Acq On : 20 Dec 2001 9:37 pm Operator: GALOS Sample : gems unknown 11/20 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

6.70 0.51 ng/uL 180885 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 / Tentative ID MW MolForm CAS# Qual

1 3-Hexanol 102 C6H140 000623-37-0 83 2 3-Hexanol 102 C6H140 000623-37-0 83 3 3-Hi xanol 102 C6H140 000623-37-0 83 4 3-a xanol 102 C6H140 _ _____000623-37-0 83 Abundance Scan 203 (6.704 min): 27951 .D (-) m/z 59.16 100.00%| 55 59

5000 73 43 s 39 ' + TT.. 6.40 680 6.80 7.00 ' ' I ' ' ' ■ I

-TT »l••’•i••>'i•" •i•• •• i •" ■ i ■ ■ ■ ■ i • • • ■ i ■ m/z 55.1.0 82.66? miz- 20 25 3035 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #1762:3-Hexanol i 59 55 31 5000 27 43 73 I ' ' ' • I • ' ' ' I 6.40 6.60 6.80 7.00 m/ z 73.0.5 39.92 ‘I‘ tumnpopr ______________ 102 ■! ■ ■ • • J ■ • • > | • ■ • - | 'I ’ '■ 'l "■• I ' " ■ l ' Mz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63527: 3-Hexanol , 59 55 i I ' ' ' ' I ' 1 1 ' I 6.40 6.60 6.80 7.00 5000- 31 73 m/z 43.10 30.51% l i 27 : 45 84 m/z-> Abundance> TTTTTTTT — ' i ■" ■ i" " i" " i" " i'1" i'1" i ’ " ‘ i ■ i1" 1 i" " I" ■' i" " i'1'1 i1"11 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 #63531:3-Hexanol 55 59 A.. — 6.40 6.60 6.80 7.00 m/z 41.10 21.77% 5000- 73 43 39 69 miz—> mmTmHTm 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Mfr TPM 6.40 6.60 6.80 7.00

27951.D NP112701.M Fri Dec 21 09:58:32 2001 Page 3

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