GCMS unknowns analysis results for sample AD27951, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C: \HPCHEM\1\DATA\DEC1901\27951.D Vial: 7 Acq On : 20 Dec 2001 9:37 pm Operator: GALOS Sample : gems unknown 11/20 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Hexanol Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

6.81 0.76 ng/uL 267394 1,4-Dichlorobenzene-d4 11.87

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexa: 1 102 C6H140 000626-93-7 83 2 2-Hex ol 102 C6H140 000626-93-7 83 3 2-He: .nol 102 C6H140 000626-93-7 83 4 2-P tanol, 4-methyl- 102 C6H140 000108-11-2 78 Abundance Scan 215(6.814 min): 27951. D(-) m/z 45.10 100.00% 45

5000 ............ I | 4 I ......... 41 69 | I l C| I l") I | I » I | I I

84 87 6.40 6.60 6.80 7.00 7.20

miz-? 10 | |■.■.| 15 20 25 30 ■ 11 ■. ■ 11 . ■ r , i r . V | L 11 +5356.. I| 35 40 45 50 55 60 65 70 TPIT TIIWTHTTTTTT 75 80 85 90 95 m/z 41.10 15.48% Abundance #63583:2-Hexanol i

5000

27 31 39 42, 45

5558 69 | 84 87 NW _ . . . 6.40 m/z 6.60 6.80 69.1.0 7.00 7.20 14.60% ......... H....... T TTTTTIIuut“pu i " ■ ■ i ■ ■" i " " i1' ■ ■ 11 ■ " i ■ "11' * •' I' miz—> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63584: 2-Hexanol 45 ... , , , | \......... 6.40 6.60 6.80 7.00 ' 7.20 ' 5000- m/z 43.10 12.46% 69 ; 19 27 31 42 56 ! 84 87

| T’’’—0uuumuuuuum—O*uuum!TTTTT miz-__ 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #1792:2-Hexanol 45 -ss 6.40 6.60 6.80 r . । i ITr|Tr 7.00 7.20 m/z 44.05 8.47% 5000

69 LAAA L , 44 A AA miz—> --31..342+ 55 58 TITTTTHT IIWWunp—TpT 84 87 10.15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 6.40 6.60 6.80 7.00 7.20

27951.D NP112701.M Fri Dec 21 09:58:34 2001 Page 4

NYC-WTC_000034070