GCMS analysis results for sample AD28165, Jan 2002

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Data File : C:\HPCHEM\1\DATA\DEC2101\28106.D Vial: 13 Acq On : 22 Dec 2001 4:51 am Operator: GALOS Sample : gems unknown 11/23 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanone Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

6.51 0.91 ng/uL 331396 1,4-Dichlorobenzene-d4 11.79

Hit# of 5 'Tentative ID MW MolForm CAS# Qua!

1 2-Hexanone 100 C6H120 000591-78-6 91 2 2-Hexanone 100 C6H120 000591-78-6 91 3 2-Hexanone 100 C6H120 000591-78-6 91 4 2-Hexanone 100 C6H120 000591-78-6 91 [Abundance Scan 182 (6.508 min): 28106.D (-) m/z 43.05 100.00% 48

5000 58

TTTTT 1 --- -. T 6.20 6.40 6.60 6.80 ____ +53 |HTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTT --38l "TTTTTTTTTTT 71 85 100 m/z 58.1.0 48.88% m/z~>___ 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63384:2-Hexanone 43

5000 58 6.20 1 TTTPr —6.40 . T T. T. T. T. 1. 1' 6.60 6.80 29 m/ z 41.10 15.37% 39 71 85 100 1’Io"I TTpT T TTTDTT +TTTTTTTTTTTNTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTT miz- 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1555; 2- Hexanone 43

6.20 6.40 6.60 6.80 58 5000 m/z 57.10 14.91%

27 39 ! 71 85 100 TTTTTTTTTTTTT — 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63386: 2-Hexanone TITT 43 6.20 6.40 6.60 6.80 m/z 100.05 8.32% 5000 58 29 I 71 85 100 miz-> TTIWTTT TTTTTTTITHTTTTTTTTTH 1111111 n 1111 n 11111TT, 11 >-| H111T । TTTTTTT m । 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 ....... —.......... 1 6.20 6.40 6.60 6.80

28106.D NP112701.M Fri Dec 28 09:55:38 2001 Page 2

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