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GCMS analysis results for sample AD27767, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD27767 for unknown compounds and surrogates on January 3, 2002.

NYC-WTC_000033358–000033372

Folder label: “GCMS X 11/16/01 A 12/18 - 12/20/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC19O1\27767.D Vial: 10 Acq On : 20 Dec 2001 4:08 am Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title 208 625/TCLP calibration table Library C: \DATABASE\NBS75K . L ********************************************************************* Peak Number 4 2-Hexanol, (R)- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

6.82 1.17 ng/uL 355754 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

. 1 2-Hexanol, (R) - 102 C6H140 026549-24-6 83 2 2-Hexanol 102 C6H140 000626-93-7 83 3 2-Hexanol, (S) - 102 C6H140 052019-78-0 74 4 2-Hexanol 'Abundance ( 102 C6H140 000626-93-7 64 Scan 216 (6.819 min): 27767.D (-) m/ z 45.10 100.00% 45

5000- - 41 69 84 87 6.40 6.60 6.80 7.00 7.20

m/z~> 3844 Tm 53 56 —ur59 1 io 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 m/ Z mmmPTTTTT i 69.10 15.07% 'Abundance #1794: 2-Hexanol, (R)- 45

5000 11000 6.40 6.60 6.80 7.00 7.20 m/ Z 41.10 14.11% 69 19 29 39 42, 55 | 84 87 ‘T‘ r...... I... 11 ■»■! TTTTTTTT 1 . 1 | I I I I | I I I I ] I I I I | , I , I | I M I | I I ■ ■ | ■ I I > | > «

_NU miz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63584: 2-Hexanol 45 I 6.40 6.60 6.80 7.00 7.20 5000 - m/ z 43.10 11.16% 69 19 27 31 42, 56 | 84 8/ TBWPIPBgur .. I.... I > ' i'''' i: 1'' i' ■ ■ ■ i'' ■ ’ i' ‘' i' ■ ‘' i ■ Dpr m/z-> Abundance 10 15 20 25 30 35 40 45 50 55 #1769: 2-Hexanol, (S) 60 65 70 75 80 85 90 95 ■ AAA....... — 45 6.40 6.60 6.80 7.00 7.20 m/z 44.10 8.13% 5000 -

m/z-> I,... .... ,4... ' ri 10 15 20 25 30 35 39 42. 4G 45 50 55 55 60 65 69 -r-rp-TT-q-rTTT^-rr-T-rp-TTIumuu‘tt—uu—n—TTi‘ 70 75 80 84 87 85 90 95 AAAMAA D / 7.00 7.20

27767.D NP112701.M Thu Dec 20 11:46:03 2001 Page 4

NYC-WTC_000033369

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