GCMS analysis results for sample AD27767, Jan 2002

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Library Search Compound Report

Data File : C : \HPCHEM\ 1 \DATA\DEC19 0127767.D Vial: 10 Acq On : 20 Dec 2001 4:08 am Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins . Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 3 3-Hexanol Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

6.71 0.88 ng/uL 267775 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanol 102 C6H140 000623-37-0 83 2 3-Hexanol • 102 C6H140 000623-37-0 83 3 3-Hexanol 102 C6H140 000623-37-0 83 4 3-Hexano 1 102 C6H140 000623-37-0 83 Abundance » Scan 204 (6.709 min): 27767.D (-) m/ z 59.10 100.00%| 55 59

5000 73 43 44 i' ■ ■ ■ i ' 1 ■ ■ i 39 6.40 6.60 6.80 7.00 m/z-> TrrrT TT —HH+ 51 +4I ” ’' I •' " I 1 1 "| 1 '"i 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 ।Tr+ T‘ m/ z 55.10 78.45% Abundance #63531:3-Hexanol 59 55

5000- 73 6.40 6.60 6.80 7.00 43 m/z 73.05 43.25%

m/z-> 20 25 rir i •" ‘ i T 39 + 69 , r1'1111" 11111 ""I "" ' "I "" I • p-m-fT 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 1I I ‘ TUIIIETT

Abundance #63528: 3-Hexanol 59 55 ! rr ' I T ♦ ' TI -I I ! I I > I I I I 6.40 6.60 6.80 7.00 73 5000 m/z 43.10 32.85% 31 I 27 45 .. 11 84 r "' i * ’ •' i'"' i" “ i iTT ' I" " I" " r ■ " i " " i1' " r '" i T / m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63529:3-Hexanol • . । ■ 1 । ' 1 ■ 1 । ■ ■ ■ < i

55 59 6.40 6.60 6.80 7.00 m/ Z 41.05 23.65%

5000- 31 __ 73 27 44 ■ ■ i ■" • i' TI m HHmm +4 TTT TT T ' । | । । | । । । TTTTT’IT I . I |102 ’ i r M | i . . i| i TII , mnnr TIBB—n/T m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 6.40 6.60 6.80 7.00 1

27767.D NP112701.M Thu Dec 20 11:46:01 2001 ’Page 3

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